Radiation furnace for synchrotron dark-field X-ray microscopy experiments

C. Yildirim*, H. Vitoux, L. E. Dresselhaus-Marais, R. Steinmann, Y. Watier, P. K. Cook, M. Kutsal, C. Detlefs

*Corresponding author for this work

Research output: Contribution to journalJournal articleResearchpeer-review

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Abstract

We present a multi-purpose radiation furnace designed for X-ray experiments at synchrotrons. The furnace is optimized specifically for dark-field X-ray microscopy (DFXM) of crystalline materials at beamline ID06 of the European Synchrotron Radiation Facility. The furnace can reach temperatures above 1200 °C with a thermal stability better than 10 °C, with heating and cooling rates up to 30 K/s. The non-contact heating design enables samples to be heated either in air or in a controlled atmosphere contained within a capillary tube. The temperature was calibrated via the thermal expansion of an α-iron grain. Temperature profiles in the y and z axes were measured by scanning a thermocouple through the focal spot of the radiation furnace. In the current configuration of the beamline, this furnace can be used for DFXM, near-field X-ray topography, bright-field X-ray nanotomography, high-resolution reciprocal space mapping, and limited powder diffraction experiments. As a first application, we present a DFXM case study on isothermal heating of a commercially pure single crystal of aluminum.
Original languageEnglish
Article number065109
JournalReview of Scientific Instruments
Volume91
Issue number6
Number of pages8
ISSN0034-6748
DOIs
Publication statusPublished - 2020

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