Preparation of iron sulphides by high energy ball milling

R. Lin; Jianzhong Jiang; R.K. Larsen; Steen Mørup; F.J. Berry

Preparation of iron sulphides by high energy ball milling

R. Lin, Jianzhong Jiang, R.K. Larsen, Steen Mørup, F.J. Berry

Department of Physics

The Open University

Research output: Contribution to journal › Journal article › Research › peer-review

Abstract

The reaction of a powder mixture consisting of 50 a.% Fe and 50 a.% S during high energy ball milling has been studied by x-ray diffraction and Mossbauer spectroscopy. After around 19 h of milling FeS2 and FeS havebeen formed. By further milling the FeS compound becomes dominating and only FeS with an average crystallite size of about 10 nm was observed after milling times longer than 67 h. Mossbauer spectra obtained with applied fields show that the particles are antiferromagnetic or have a strongly canted spin structure.

Original language	English
Journal	Hyperfine Interactions (C)
Volume	3
Pages (from-to)	45-
Publication status	Published - 1998

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title = "Preparation of iron sulphides by high energy ball milling",

abstract = "The reaction of a powder mixture consisting of 50 a.% Fe and 50 a.% S during high energy ball milling has been studied by x-ray diffraction and Mossbauer spectroscopy. After around 19 h of milling FeS2 and FeS havebeen formed. By further milling the FeS compound becomes dominating and only FeS with an average crystallite size of about 10 nm was observed after milling times longer than 67 h. Mossbauer spectra obtained with applied fields show that the particles are antiferromagnetic or have a strongly canted spin structure.",

author = "R. Lin and Jianzhong Jiang and R.K. Larsen and Steen M{\o}rup and F.J. Berry",

year = "1998",

language = "English",

volume = "3",

pages = "45--",

journal = "Hyperfine Interactions (C)",

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TY - JOUR

T1 - Preparation of iron sulphides by high energy ball milling

AU - Lin, R.

AU - Jiang, Jianzhong

AU - Larsen, R.K.

AU - Mørup, Steen

AU - Berry, F.J.

PY - 1998

Y1 - 1998

N2 - The reaction of a powder mixture consisting of 50 a.% Fe and 50 a.% S during high energy ball milling has been studied by x-ray diffraction and Mossbauer spectroscopy. After around 19 h of milling FeS2 and FeS havebeen formed. By further milling the FeS compound becomes dominating and only FeS with an average crystallite size of about 10 nm was observed after milling times longer than 67 h. Mossbauer spectra obtained with applied fields show that the particles are antiferromagnetic or have a strongly canted spin structure.

AB - The reaction of a powder mixture consisting of 50 a.% Fe and 50 a.% S during high energy ball milling has been studied by x-ray diffraction and Mossbauer spectroscopy. After around 19 h of milling FeS2 and FeS havebeen formed. By further milling the FeS compound becomes dominating and only FeS with an average crystallite size of about 10 nm was observed after milling times longer than 67 h. Mossbauer spectra obtained with applied fields show that the particles are antiferromagnetic or have a strongly canted spin structure.

M3 - Journal article

VL - 3

SP - 45-

JO - Hyperfine Interactions (C)

JF - Hyperfine Interactions (C)

ER -