Methodology for in situ synchrotron X-ray studies in the laser-heated diamond anvil cell

M. Mezouar; R. Giampaoli; G. Garbarino; I. Kantor; A. Dewaele; G. Weck; S. Boccato; V. Svitlyk; A. D. Rosa; R. Torchio; O. Mathon; O. Hignette; S. Bauchau

doi:10.1080/08957959.2017.1306626

Methodology for in situ synchrotron X-ray studies in the laser-heated diamond anvil cell

M. Mezouar^*, R. Giampaoli, G. Garbarino, I. Kantor, A. Dewaele, G. Weck, S. Boccato, V. Svitlyk, A. D. Rosa, R. Torchio, O. Mathon, O. Hignette, S. Bauchau

^*Corresponding author for this work

Department of Physics

Research output: Contribution to journal › Journal article › Research › peer-review

Abstract

A review of some important technical challenges related to in situ diamond anvil cell laser heating experimentation at synchrotron X-ray sources is presented. The problem of potential chemical reactions between the sample and the pressure medium or the carbon from the diamond anvils is illustrated in the case of elemental tantalum. Preliminary results of a comparison between reflective and refractive optics for high temperature measurements in the laser-heated diamond anvil cell are briefly discussed. Finally, the importance of the size and relative alignment of X-ray and laser beams for quantitative X-ray measurements is presented.

Original language	English
Journal	High Pressure Research
Volume	37
Issue number	2
Pages (from-to)	170-180
Number of pages	11
ISSN	0895-7959
DOIs	https://doi.org/10.1080/08957959.2017.1306626
Publication status	Published - 3 Apr 2017

Keywords

chemical reactions
diamond anvil cells
Laser heating
temperature measurements
X-rays

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10.1080/08957959.2017.1306626

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title = "Methodology for in situ synchrotron X-ray studies in the laser-heated diamond anvil cell",

abstract = "A review of some important technical challenges related to in situ diamond anvil cell laser heating experimentation at synchrotron X-ray sources is presented. The problem of potential chemical reactions between the sample and the pressure medium or the carbon from the diamond anvils is illustrated in the case of elemental tantalum. Preliminary results of a comparison between reflective and refractive optics for high temperature measurements in the laser-heated diamond anvil cell are briefly discussed. Finally, the importance of the size and relative alignment of X-ray and laser beams for quantitative X-ray measurements is presented.",

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AU - Mezouar, M.

AU - Giampaoli, R.

AU - Garbarino, G.

AU - Kantor, I.

AU - Dewaele, A.

AU - Weck, G.

AU - Boccato, S.

AU - Svitlyk, V.

AU - Rosa, A. D.

AU - Torchio, R.

AU - Mathon, O.

AU - Hignette, O.

AU - Bauchau, S.

PY - 2017/4/3

Y1 - 2017/4/3

N2 - A review of some important technical challenges related to in situ diamond anvil cell laser heating experimentation at synchrotron X-ray sources is presented. The problem of potential chemical reactions between the sample and the pressure medium or the carbon from the diamond anvils is illustrated in the case of elemental tantalum. Preliminary results of a comparison between reflective and refractive optics for high temperature measurements in the laser-heated diamond anvil cell are briefly discussed. Finally, the importance of the size and relative alignment of X-ray and laser beams for quantitative X-ray measurements is presented.

AB - A review of some important technical challenges related to in situ diamond anvil cell laser heating experimentation at synchrotron X-ray sources is presented. The problem of potential chemical reactions between the sample and the pressure medium or the carbon from the diamond anvils is illustrated in the case of elemental tantalum. Preliminary results of a comparison between reflective and refractive optics for high temperature measurements in the laser-heated diamond anvil cell are briefly discussed. Finally, the importance of the size and relative alignment of X-ray and laser beams for quantitative X-ray measurements is presented.

KW - chemical reactions

KW - diamond anvil cells

KW - Laser heating

KW - temperature measurements

KW - X-rays

U2 - 10.1080/08957959.2017.1306626

DO - 10.1080/08957959.2017.1306626

M3 - Journal article

AN - SCOPUS:85016507248

SN - 0895-7959

VL - 37

SP - 170

EP - 180

JO - High Pressure Research

JF - High Pressure Research

IS - 2

ER -

Methodology for in situ synchrotron X-ray studies in the laser-heated diamond anvil cell

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Keywords

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