Mechanochemical synthesis of Fe-S materials.

Jianzhong Jiang; R.K. Larsen; R. Lin; Steen Mørup; Ib Chorkendorff; K. Nielsen; Kent Kammer Hansen; Keld West

doi:10.1006/jssc.1998.7761

Mechanochemical synthesis of Fe-S materials.

Jianzhong Jiang
, R.K. Larsen
, R. Lin
, Steen Mørup
, Ib Chorkendorff
, K. Nielsen
, Kent Kammer Hansen
, Keld West

Research output: Contribution to journal › Journal article › Research › peer-review

Abstract

Powder mixtures of metallic iron and sulfur have been milled in a high-energy planetary ball mill and the formation of iron sulfides has been studied by x-ray diffraction, Mossbauer spectroscopy, and scanning electron microscopy. For Fe:S ratios of 1:1 and 1:2 the final products are FeS with the modified NiAs structure and FeS2 (pyrite), respectively. No other iron sulfides were formed for any of the Fe:S ratios studied. The FeS phase has been tested as an electrode material in lithium batteries.

Original language	English
Journal	Journal of Solid State Chemistry
Volume	138
Issue number	1
Pages (from-to)	114-125
ISSN	0022-4596
DOIs	https://doi.org/10.1006/jssc.1998.7761
Publication status	Published - 1998

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title = "Mechanochemical synthesis of Fe-S materials.",

abstract = "Powder mixtures of metallic iron and sulfur have been milled in a high-energy planetary ball mill and the formation of iron sulfides has been studied by x-ray diffraction, Mossbauer spectroscopy, and scanning electron microscopy. For Fe:S ratios of 1:1 and 1:2 the final products are FeS with the modified NiAs structure and FeS2 (pyrite), respectively. No other iron sulfides were formed for any of the Fe:S ratios studied. The FeS phase has been tested as an electrode material in lithium batteries.",

author = "Jianzhong Jiang and R.K. Larsen and R. Lin and Steen M{\o}rup and Ib Chorkendorff and K. Nielsen and \{Kammer Hansen\}, Kent and Keld West",

year = "1998",

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journal = "Journal of Solid State Chemistry",

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T1 - Mechanochemical synthesis of Fe-S materials.

AU - Jiang, Jianzhong

AU - Larsen, R.K.

AU - Lin, R.

AU - Mørup, Steen

AU - Chorkendorff, Ib

AU - Nielsen, K.

AU - Kammer Hansen, Kent

AU - West, Keld

PY - 1998

Y1 - 1998

N2 - Powder mixtures of metallic iron and sulfur have been milled in a high-energy planetary ball mill and the formation of iron sulfides has been studied by x-ray diffraction, Mossbauer spectroscopy, and scanning electron microscopy. For Fe:S ratios of 1:1 and 1:2 the final products are FeS with the modified NiAs structure and FeS2 (pyrite), respectively. No other iron sulfides were formed for any of the Fe:S ratios studied. The FeS phase has been tested as an electrode material in lithium batteries.

AB - Powder mixtures of metallic iron and sulfur have been milled in a high-energy planetary ball mill and the formation of iron sulfides has been studied by x-ray diffraction, Mossbauer spectroscopy, and scanning electron microscopy. For Fe:S ratios of 1:1 and 1:2 the final products are FeS with the modified NiAs structure and FeS2 (pyrite), respectively. No other iron sulfides were formed for any of the Fe:S ratios studied. The FeS phase has been tested as an electrode material in lithium batteries.

U2 - 10.1006/jssc.1998.7761

DO - 10.1006/jssc.1998.7761

M3 - Journal article

SN - 0022-4596

VL - 138

SP - 114

EP - 125

JO - Journal of Solid State Chemistry

JF - Journal of Solid State Chemistry

IS - 1

ER -

Mechanochemical synthesis of Fe-S materials.

Abstract

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