Measurements of local chemistry and structure in Ni(O)-YSZ composites during reduction using energy-filtered environmental TEM

Quentin Jeangros, Thomas Willum Hansen, Jakob Birkedal Wagner, Rafal E. Dunin-Borkowski, Cecile Hebert, Jan Van herle, Aicha Hessler-Wyser

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    Abstract

    Energy-filtered transmission electron microscopy images are acquired during the reduction of a NiO-YSZ composite in H-2 up to 600 degrees C. Temperature-resolved quantitative information about both chemistry and structure is extracted with nm spatial resolution from the data, paving the way for the development of detailed reduction models.
    Original languageEnglish
    JournalChemical Communications
    Volume50
    Issue number15
    Pages (from-to)1808-1810
    Number of pages3
    ISSN1359-7345
    DOIs
    Publication statusPublished - 2014

    Bibliographical note

    ©The Royal Society of Chemistry 2014

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