High and Low Temperature Surface Hardening of Martensitic Stainless Steels

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Abstract

In the present work high and low temperature surface hardening of X30Cr13 (AISI 420) martensitic stainless steel is addressed. In particular, high temperature solution nitriding (HTSN) of thin samples is investigated. The use of thin samples makes it possible to obtain fully homogenous materials. Three different nitrogen partial pressures were analysed, leading to three different equilibrium nitrogen contents and resulting microstructures. This makes it possible to investigate the nitrogen absorption as a function of partial pressure and the fraction of retained austenite as a function of nitrogen content. Moreover, low temperature surface hardening (LTSH) by means of gaseous nitriding in NH3 was carried out on the three HTSN microstructures at different temperatures. Thus, insight is obtained in the combining high and low temperature surface hardening for optimizing the performance of the steel with respect to fatigue and wear, without impairing, but preferably improving, the corrosion performance. Additionally, the experiments offer information on the effect of the heat treatment cycle (thermal impact). ThermoCalc was applied adjust the appropriate HTSN parameters. Reflected light microscopy and X-ray diffraction are applied for the characterization of the morphology and phase constitution of the developing case. Micro-Vickers indentation provides information on the depth dependence of the hardness.
Original languageEnglish
Publication date2019
Number of pages10
Publication statusPublished - 2019
EventESSC & DUPLEX 2019 - Vienna, Austria
Duration: 30 Sep 20192 Oct 2019

Conference

ConferenceESSC & DUPLEX 2019
CountryAustria
CityVienna
Period30/09/201902/10/2019

Keywords

  • Martensitic stainless steel
  • Low temperature surface hardening
  • Gas nitriding
  • High temperature solution nitriding
  • Hardness depth profile
  • X-ray diffraction

Cite this

@conference{2b032b21606c48c48660e26aa6acf136,
title = "High and Low Temperature Surface Hardening of Martensitic Stainless Steels",
abstract = "In the present work high and low temperature surface hardening of X30Cr13 (AISI 420) martensitic stainless steel is addressed. In particular, high temperature solution nitriding (HTSN) of thin samples is investigated. The use of thin samples makes it possible to obtain fully homogenous materials. Three different nitrogen partial pressures were analysed, leading to three different equilibrium nitrogen contents and resulting microstructures. This makes it possible to investigate the nitrogen absorption as a function of partial pressure and the fraction of retained austenite as a function of nitrogen content. Moreover, low temperature surface hardening (LTSH) by means of gaseous nitriding in NH3 was carried out on the three HTSN microstructures at different temperatures. Thus, insight is obtained in the combining high and low temperature surface hardening for optimizing the performance of the steel with respect to fatigue and wear, without impairing, but preferably improving, the corrosion performance. Additionally, the experiments offer information on the effect of the heat treatment cycle (thermal impact). ThermoCalc was applied adjust the appropriate HTSN parameters. Reflected light microscopy and X-ray diffraction are applied for the characterization of the morphology and phase constitution of the developing case. Micro-Vickers indentation provides information on the depth dependence of the hardness.",
keywords = "Martensitic stainless steel, Low temperature surface hardening, Gas nitriding, High temperature solution nitriding, Hardness depth profile, X-ray diffraction",
author = "Chiara Tibollo and Matteo Villa and Christiansen, {Thomas L.} and Somers, {Marcel A. J.}",
year = "2019",
language = "English",
note = "ESSC & DUPLEX 2019 ; Conference date: 30-09-2019 Through 02-10-2019",

}

High and Low Temperature Surface Hardening of Martensitic Stainless Steels. / Tibollo, Chiara; Villa, Matteo; Christiansen, Thomas L.; Somers, Marcel A. J.

2019. Abstract from ESSC & DUPLEX 2019, Vienna, Austria.

Research output: Contribution to conferenceConference abstract for conferenceResearchpeer-review

TY - ABST

T1 - High and Low Temperature Surface Hardening of Martensitic Stainless Steels

AU - Tibollo, Chiara

AU - Villa, Matteo

AU - Christiansen, Thomas L.

AU - Somers, Marcel A. J.

PY - 2019

Y1 - 2019

N2 - In the present work high and low temperature surface hardening of X30Cr13 (AISI 420) martensitic stainless steel is addressed. In particular, high temperature solution nitriding (HTSN) of thin samples is investigated. The use of thin samples makes it possible to obtain fully homogenous materials. Three different nitrogen partial pressures were analysed, leading to three different equilibrium nitrogen contents and resulting microstructures. This makes it possible to investigate the nitrogen absorption as a function of partial pressure and the fraction of retained austenite as a function of nitrogen content. Moreover, low temperature surface hardening (LTSH) by means of gaseous nitriding in NH3 was carried out on the three HTSN microstructures at different temperatures. Thus, insight is obtained in the combining high and low temperature surface hardening for optimizing the performance of the steel with respect to fatigue and wear, without impairing, but preferably improving, the corrosion performance. Additionally, the experiments offer information on the effect of the heat treatment cycle (thermal impact). ThermoCalc was applied adjust the appropriate HTSN parameters. Reflected light microscopy and X-ray diffraction are applied for the characterization of the morphology and phase constitution of the developing case. Micro-Vickers indentation provides information on the depth dependence of the hardness.

AB - In the present work high and low temperature surface hardening of X30Cr13 (AISI 420) martensitic stainless steel is addressed. In particular, high temperature solution nitriding (HTSN) of thin samples is investigated. The use of thin samples makes it possible to obtain fully homogenous materials. Three different nitrogen partial pressures were analysed, leading to three different equilibrium nitrogen contents and resulting microstructures. This makes it possible to investigate the nitrogen absorption as a function of partial pressure and the fraction of retained austenite as a function of nitrogen content. Moreover, low temperature surface hardening (LTSH) by means of gaseous nitriding in NH3 was carried out on the three HTSN microstructures at different temperatures. Thus, insight is obtained in the combining high and low temperature surface hardening for optimizing the performance of the steel with respect to fatigue and wear, without impairing, but preferably improving, the corrosion performance. Additionally, the experiments offer information on the effect of the heat treatment cycle (thermal impact). ThermoCalc was applied adjust the appropriate HTSN parameters. Reflected light microscopy and X-ray diffraction are applied for the characterization of the morphology and phase constitution of the developing case. Micro-Vickers indentation provides information on the depth dependence of the hardness.

KW - Martensitic stainless steel

KW - Low temperature surface hardening

KW - Gas nitriding

KW - High temperature solution nitriding

KW - Hardness depth profile

KW - X-ray diffraction

M3 - Conference abstract for conference

ER -