TY - JOUR
T1 - Estimation of the sensory properties of black tea samples using non-destructive near-infrared spectroscopy sensors
AU - Turgut, Sebahattin Serhat
AU - Entrenas, José Antonio
AU - Taşkın, Emre
AU - Garrido-Varo, Ana
AU - Pérez-Marín, Dolores
PY - 2022
Y1 - 2022
N2 - The quality characteristics of black tea are routinely assessed before it is purchased, blended and marketed to ensure its quality and value. Although some of these quality characteristics can be measured analytically, others need to be determined as sensory scores following cupping tests conducted by tea experts. However, most of these analyses (especially the sensory ones) require high training and expertise, are time-consuming and prone to human error. Therefore, in this study, non-destructive spectral sensors were combined with chemometric methods to rapidly measure the results of the cupping test (appearance, body, colour and overall quality) and some other important sensory quality attributes (bulk density, cellulose, water extract and moisture) of black tea samples. A total of 54 black tea samples from Türkiye were analysed in three different NIRS (near-infrared spectroscopy) devices (MicroNIR™ 1700, Matrix-F FT-NIR and NIRS DS 2500). Partial Least Squares Regression (PLSR) and Principal Components Regression (PCR) with stepwise variable elimination were used as regression algorithms to develop the NIR calibrations. As a result, PLSR provided slightly superior estimates with R2cv between 0.83 and 0.97 and RPDcv between 2.47 and 5.79 for sensory traits. For analytical traits, model statistics for PLSR ranged between 0.66-0.89 and 1.72–3.08 for R2cv and RPDcv, respectively. These results suggest that PLSR combined with FT-NIR technology may be promising for rapid and economical evaluation of sensory (cupping test) scores and related properties for its use in the tea industry.
AB - The quality characteristics of black tea are routinely assessed before it is purchased, blended and marketed to ensure its quality and value. Although some of these quality characteristics can be measured analytically, others need to be determined as sensory scores following cupping tests conducted by tea experts. However, most of these analyses (especially the sensory ones) require high training and expertise, are time-consuming and prone to human error. Therefore, in this study, non-destructive spectral sensors were combined with chemometric methods to rapidly measure the results of the cupping test (appearance, body, colour and overall quality) and some other important sensory quality attributes (bulk density, cellulose, water extract and moisture) of black tea samples. A total of 54 black tea samples from Türkiye were analysed in three different NIRS (near-infrared spectroscopy) devices (MicroNIR™ 1700, Matrix-F FT-NIR and NIRS DS 2500). Partial Least Squares Regression (PLSR) and Principal Components Regression (PCR) with stepwise variable elimination were used as regression algorithms to develop the NIR calibrations. As a result, PLSR provided slightly superior estimates with R2cv between 0.83 and 0.97 and RPDcv between 2.47 and 5.79 for sensory traits. For analytical traits, model statistics for PLSR ranged between 0.66-0.89 and 1.72–3.08 for R2cv and RPDcv, respectively. These results suggest that PLSR combined with FT-NIR technology may be promising for rapid and economical evaluation of sensory (cupping test) scores and related properties for its use in the tea industry.
KW - Cupping test
KW - NIR chemometric Models
KW - Python
KW - Non-destructive sensors
KW - PCR
KW - PLSR
U2 - 10.1016/j.foodcont.2022.109260
DO - 10.1016/j.foodcont.2022.109260
M3 - Journal article
SN - 0956-7135
VL - 142
JO - Food Control
JF - Food Control
M1 - 109260
ER -