Editing of H2BC NMR spectra

NT Nyberg, Jens Øllgaard Duus, OW Sorensen

Research output: Contribution to journalJournal articleResearchpeer-review

Abstract

New versions of the H2BC pulse sequence (Nyberg NT, Duus JO, Sorensen OW. J. Am. Chem. Soc. 2005; 127: 6154) that edit into two subspectra according to the number of protons attached to C-13 nuclei being odd or even are introduced. These sequences can be useful for resolving spectral overlap, which is demonstrated on the molecule prednisolone [(11 beta)-11,17,21-trihydroxypregna-1,4-diene-3,20-dione]. Copyright (c) 2005 John Wiley & Sons, Ltd.
Original languageEnglish
JournalMagnetic Resonance in Chemistry
Volume43
Issue number12
Pages (from-to)971-974
Number of pages4
ISSN0749-1581
DOIs
Publication statusPublished - 2005
Externally publishedYes

Keywords

  • CHEMISTRY,
  • SPECTROSCOPY
  • CARBON SKELETON
  • SENSITIVITY
  • INADEQUATE
  • NMR
  • H-1
  • C-13
  • H2BC
  • prednisolone
  • Magnetic Resonance Spectroscopy
  • Prednisolone
  • 9PHQ9Y1OLM Prednisolone
  • article
  • chemistry
  • methodology
  • nuclear magnetic resonance spectroscopy
  • 13C
  • 1H

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