Direct measurements of the magnetic entropy change

Kaspar Kirstein Nielsen, Henrique Neves Bez, Lars von Moos, Rasmus Bjørk, Dan Eriksen, Christian Bahl

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Abstract

An experimental device that can accurately measure the magnetic entropy change, Δs, as a function of temperature, T, and magnetic field, H, is presented. The magnetic field source is in this case a set of counter-rotating concentric Halbach-type magnets, which produce a highly homogeneous applied field with constant orientation. The field may be varied from 0 to 1.5 T in a continuous way. The temperature stability of the system is controlled to within ±10 mK and the standard range for the current setup is from 230 K to 330 K. The device is under high vacuum and we show that thermal losses to the ambient are negligible in terms of the calorimetric determination of the magnetic entropy change, while the losses cannot be ignored when correcting for the actual sample temperature. We apply the device to two different types of samples; one is commercial grade Gd, i.e., a pure second-order phase transition material, while the other is Gd5Si2Ge2, a first order magnetic phase transition material. We demonstrate the device’s ability to fully capture the thermal hysteresis of the latter sample by following appropriate thermal resetting scheme and magnetic resetting scheme. © 2015 AIP Publishing LLC.
Original languageEnglish
Article number103903
JournalReview of Scientific Instruments
Volume86
Issue number10
Number of pages6
ISSN0034-6748
DOIs
Publication statusPublished - 2015

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