Development of an Intensified Reactive Distillation Process for the Synthesis of Dioxolane Products

Arick  Castillo-Landero; Arturo  Jiménez-Gutiérreza; Rafiqul Gani

doi:10.1016/B978-0-444-63965-3.50182-3

Development of an Intensified Reactive Distillation Process for the Synthesis of Dioxolane Products

Arick Castillo-Landero
, Arturo Jiménez-Gutiérreza
, Rafiqul Gani

Instituto Tecnológico de Celaya

Research output: Chapter in Book/Report/Conference proceeding › Article in proceedings › Research › peer-review

Abstract

A methodology for process intensification that reduces the number of pieces of equipment as part of the design of a chemical process is presented. The method is based on three stages, the first one to detect feasible process alternatives, the second one to identify intensification opportunities, and in the third one phenomena building blocks are used to develop the best intensified process. The methodology is applied for the intensification of an aldolization process for the synthesis of dioxolane products, based on reacting ethylene glycol and 1,2-butanediol with acetaldehyde to produce 2-methyl,1,3-dioxolane (2MD) and 4-ethyl,2-methyl,1,3-dioxolane (4EMD). It is shown how a base flowsheet is effectively converted into an intensified reactive distillation process with the application of the intensification methodology.

Original language	English
Title of host publication	Proceedings of the 27th European Symposium on Computer Aided Process Engineering – ESCAPE 27
Editors	Antonio Espuña, Moisès Graells, Luis Puigjaner
Volume	40
Publisher	Elsevier
Publication date	2017
Pages	1081-1086
ISBN (Electronic)	978-0-444-63965-3
DOIs	https://doi.org/10.1016/B978-0-444-63965-3.50182-3
Publication status	Published - 2017
Event	27th European Symposium on Computer Aided Process Engineering - Barcelona, Spain Duration: 1 Oct 2017 → 5 Oct 2017 Conference number: 27 https://www.elsevier.com/books/27th-european-symposium-on-computer-aided-process-engineering/espuna/978-0-444-63965-3

Conference

Conference	27th European Symposium on Computer Aided Process Engineering
Number	27
Country/Territory	Spain
City	Barcelona
Period	01/10/2017 → 05/10/2017
Internet address	https://www.elsevier.com/books/27th-european-symposium-on-computer-aided-process-engineering/espuna/978-0-444-63965-3

Series	Computer Aided Chemical Engineering
ISSN	1570-7946

Keywords

Dioxolane
Aldolization
Reactive distillation
Process intensification

Access to Document

10.1016/B978-0-444-63965-3.50182-3

OpenUrl availability

Check availability in DTU Findit

Cite this

Castillo-Landero, A., Jiménez-Gutiérreza, A., & Gani, R. (2017). Development of an Intensified Reactive Distillation Process for the Synthesis of Dioxolane Products. In A. Espuña, M. Graells, & L. Puigjaner (Eds.), Proceedings of the 27th European Symposium on Computer Aided Process Engineering – ESCAPE 27 (Vol. 40, pp. 1081-1086). Elsevier. https://doi.org/10.1016/B978-0-444-63965-3.50182-3

Castillo-Landero, Arick ; Jiménez-Gutiérreza, Arturo ; Gani, Rafiqul. / Development of an Intensified Reactive Distillation Process for the Synthesis of Dioxolane Products. Proceedings of the 27th European Symposium on Computer Aided Process Engineering – ESCAPE 27. editor / Antonio Espuña ; Moisès Graells ; Luis Puigjaner. Vol. 40 Elsevier, 2017. pp. 1081-1086 (Computer Aided Chemical Engineering).

@inproceedings{eaf28cfe8e194b8da80aa3f8461a4f2a,

title = "Development of an Intensified Reactive Distillation Process for the Synthesis of Dioxolane Products",

abstract = "A methodology for process intensification that reduces the number of pieces of equipment as part of the design of a chemical process is presented. The method is based on three stages, the first one to detect feasible process alternatives, the second one to identify intensification opportunities, and in the third one phenomena building blocks are used to develop the best intensified process. The methodology is applied for the intensification of an aldolization process for the synthesis of dioxolane products, based on reacting ethylene glycol and 1,2-butanediol with acetaldehyde to produce 2-methyl,1,3-dioxolane (2MD) and 4-ethyl,2-methyl,1,3-dioxolane (4EMD). It is shown how a base flowsheet is effectively converted into an intensified reactive distillation process with the application of the intensification methodology.",

keywords = "Dioxolane, Aldolization, Reactive distillation, Process intensification",

author = "Arick Castillo-Landero and Arturo Jim{\'e}nez-Guti{\'e}rreza and Rafiqul Gani",

year = "2017",

doi = "10.1016/B978-0-444-63965-3.50182-3",

language = "English",

volume = "40",

series = "Computer Aided Chemical Engineering",

publisher = "Elsevier",

pages = "1081--1086",

editor = "Espu{\~n}a, \{Antonio \} and Graells, \{Mois{\`e}s \} and Puigjaner, \{Luis \}",

booktitle = "Proceedings of the 27th European Symposium on Computer Aided Process Engineering {\textendash} ESCAPE 27",

address = "United Kingdom",

note = "27th European Symposium on Computer Aided Process Engineering, ESCAPE 27 ; Conference date: 01-10-2017 Through 05-10-2017",

url = "https://www.elsevier.com/books/27th-european-symposium-on-computer-aided-process-engineering/espuna/978-0-444-63965-3",

}

Castillo-Landero, A, Jiménez-Gutiérreza, A & Gani, R 2017, Development of an Intensified Reactive Distillation Process for the Synthesis of Dioxolane Products. in A Espuña, M Graells & L Puigjaner (eds), Proceedings of the 27th European Symposium on Computer Aided Process Engineering – ESCAPE 27. vol. 40, Elsevier, Computer Aided Chemical Engineering, pp. 1081-1086, 27th European Symposium on Computer Aided Process Engineering, Barcelona, Spain, 01/10/2017. https://doi.org/10.1016/B978-0-444-63965-3.50182-3

Development of an Intensified Reactive Distillation Process for the Synthesis of Dioxolane Products. / Castillo-Landero, Arick ; Jiménez-Gutiérreza, Arturo ; Gani, Rafiqul.
Proceedings of the 27th European Symposium on Computer Aided Process Engineering – ESCAPE 27. ed. / Antonio Espuña; Moisès Graells; Luis Puigjaner. Vol. 40 Elsevier, 2017. p. 1081-1086 (Computer Aided Chemical Engineering).

Research output: Chapter in Book/Report/Conference proceeding › Article in proceedings › Research › peer-review

TY - GEN

T1 - Development of an Intensified Reactive Distillation Process for the Synthesis of Dioxolane Products

AU - Castillo-Landero, Arick

AU - Jiménez-Gutiérreza, Arturo

AU - Gani, Rafiqul

N1 - Conference code: 27

PY - 2017

Y1 - 2017

N2 - A methodology for process intensification that reduces the number of pieces of equipment as part of the design of a chemical process is presented. The method is based on three stages, the first one to detect feasible process alternatives, the second one to identify intensification opportunities, and in the third one phenomena building blocks are used to develop the best intensified process. The methodology is applied for the intensification of an aldolization process for the synthesis of dioxolane products, based on reacting ethylene glycol and 1,2-butanediol with acetaldehyde to produce 2-methyl,1,3-dioxolane (2MD) and 4-ethyl,2-methyl,1,3-dioxolane (4EMD). It is shown how a base flowsheet is effectively converted into an intensified reactive distillation process with the application of the intensification methodology.

AB - A methodology for process intensification that reduces the number of pieces of equipment as part of the design of a chemical process is presented. The method is based on three stages, the first one to detect feasible process alternatives, the second one to identify intensification opportunities, and in the third one phenomena building blocks are used to develop the best intensified process. The methodology is applied for the intensification of an aldolization process for the synthesis of dioxolane products, based on reacting ethylene glycol and 1,2-butanediol with acetaldehyde to produce 2-methyl,1,3-dioxolane (2MD) and 4-ethyl,2-methyl,1,3-dioxolane (4EMD). It is shown how a base flowsheet is effectively converted into an intensified reactive distillation process with the application of the intensification methodology.

KW - Dioxolane

KW - Aldolization

KW - Reactive distillation

KW - Process intensification

U2 - 10.1016/B978-0-444-63965-3.50182-3

DO - 10.1016/B978-0-444-63965-3.50182-3

M3 - Article in proceedings

VL - 40

T3 - Computer Aided Chemical Engineering

SP - 1081

EP - 1086

BT - Proceedings of the 27th European Symposium on Computer Aided Process Engineering – ESCAPE 27

A2 - Espuña, Antonio

A2 - Graells, Moisès

A2 - Puigjaner, Luis

PB - Elsevier

T2 - 27th European Symposium on Computer Aided Process Engineering

Y2 - 1 October 2017 through 5 October 2017

ER -

Castillo-Landero A, Jiménez-Gutiérreza A, Gani R. Development of an Intensified Reactive Distillation Process for the Synthesis of Dioxolane Products. In Espuña A, Graells M, Puigjaner L, editors, Proceedings of the 27th European Symposium on Computer Aided Process Engineering – ESCAPE 27. Vol. 40. Elsevier. 2017. p. 1081-1086. (Computer Aided Chemical Engineering). doi: 10.1016/B978-0-444-63965-3.50182-3

Development of an Intensified Reactive Distillation Process for the Synthesis of Dioxolane Products

Abstract

Conference

Keywords

Access to Document

OpenUrl availability

Fingerprint

Cite this