Design of sample holder for in operando XAS of oxidation state changes in La1−xSrxMnO3±δ electrodes

Marie Lund Traulsen

doi:10.1088/1742-6596/499/1/012010

Design of sample holder for in operando XAS of oxidation state changes in La_1−xSr_xMnO_3±δ electrodes

Marie Lund Traulsen

Department of Energy Conversion and Storage

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Abstract

The design and construction of a sample holder for in operando X-ray absorption spectroscopy on solid oxide electrodes, like for instance the lanthanum strontium manganite electrodes, is explained. The sample holder is mounted in a test-cell, which is also described together with some preliminary test-results from temperature measurements and electrochemical characterisation performed on a "dummy" sample in the test cell. The test-cell is a modified version of a test-cell previously designed in our laboratory, and will in the future be used for X-ray absorption experiments on solid oxide electrodes.

Original language	English
Article number	012010
Book series	Journal of Physics: Conference Series (Online)
Volume	499
Issue number	1
Number of pages	6
ISSN	1742-6596
DOIs	https://doi.org/10.1088/1742-6596/499/1/012010
Publication status	Published - 2014
Event	22nd International Congress on X-Ray Optics and Microanalysis - University of Hamburg, Hamburg, Germany Duration: 2 Sept 2013 → 6 Sept 2013 Conference number: 22 http://www.icxom22.de/

Conference

Conference	22nd International Congress on X-Ray Optics and Microanalysis
Number	22
Location	University of Hamburg
Country/Territory	Germany
City	Hamburg
Period	02/09/2013 → 06/09/2013
Internet address	http://www.icxom22.de/

Bibliographical note

Content from this work may be used under the terms of the Creative Commons Attribution 3.0 licence. Any further distribution of this work must maintain attribution to the author(s) and the title of the work, journal citation and DOI. Published under licence by IOP Publishing Ltd

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abstract = "The design and construction of a sample holder for in operando X-ray absorption spectroscopy on solid oxide electrodes, like for instance the lanthanum strontium manganite electrodes, is explained. The sample holder is mounted in a test-cell, which is also described together with some preliminary test-results from temperature measurements and electrochemical characterisation performed on a {"}dummy{"} sample in the test cell. The test-cell is a modified version of a test-cell previously designed in our laboratory, and will in the future be used for X-ray absorption experiments on solid oxide electrodes.",

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AB - The design and construction of a sample holder for in operando X-ray absorption spectroscopy on solid oxide electrodes, like for instance the lanthanum strontium manganite electrodes, is explained. The sample holder is mounted in a test-cell, which is also described together with some preliminary test-results from temperature measurements and electrochemical characterisation performed on a "dummy" sample in the test cell. The test-cell is a modified version of a test-cell previously designed in our laboratory, and will in the future be used for X-ray absorption experiments on solid oxide electrodes.

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DO - 10.1088/1742-6596/499/1/012010

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