Combined Colorimetric and Gravimetric CMUT Sensor for Detection of Phenylacetone

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    Abstract

    The detection of phenylacetone is of interest as it is a common precursor for the synthesis of (meth)amphetamine. Resonant gravimetric sensors can be used to detect the mass and hereby the concentration of a gas while colorimetric arrays typically have an exceptional selectivity to the target analyte if the right colorimetric dyes are chosen. We present a sensor system consisting of a Capacitive Micromachined Ultrasonic Transducer (CMUT) and a colorimetric array for detection of phenylacetone. The CMUT is used as a resonant gravimetric gas sensor where the resonance frequency shift due to mass loading of the plate. A single Local Oxidation of Silicon (LOCOS) step was used to define the cavities which were sealed with a Si3N4 plate with a thickness of 100nm, resulting in a resonance frequency of 38:8MHz and a theoretical mass sensitivity of 28:3 zg/Hz·μ2. The CMUTs were functionalized with the same dyes used to fabricate colorimetric arrays. While both the CMUTs and the colorimetric arrays showed selectivity to phenylacetone, the best selectivity was achieved by the colorimetric array. Furthermore, the mass of the phenylacetone was found as a function of time. Thus, the combination of the colorimetric array and the CMUT results in a good selectivity and a quantitative value for the mass.
    Original languageEnglish
    Title of host publication2017 IEEE International Ultrasonics Symposium (IUS)
    Number of pages4
    PublisherIEEE
    Publication date2017
    ISBN (Electronic)978-1-5386-3383-0
    DOIs
    Publication statusPublished - 2017
    Event2017 IEEE International Ultrasonics Symposium (IUS) - Omni Shoreham Hotel, Washington, United States
    Duration: 6 Sep 20179 Sep 2017
    http://ewh.ieee.org/conf/ius/2017/

    Conference

    Conference2017 IEEE International Ultrasonics Symposium (IUS)
    LocationOmni Shoreham Hotel
    CountryUnited States
    CityWashington
    Period06/09/201709/09/2017
    Internet address

    Cite this

    @inproceedings{0f29b48abb3a48f78114d55350e4b679,
    title = "Combined Colorimetric and Gravimetric CMUT Sensor for Detection of Phenylacetone",
    abstract = "The detection of phenylacetone is of interest as it is a common precursor for the synthesis of (meth)amphetamine. Resonant gravimetric sensors can be used to detect the mass and hereby the concentration of a gas while colorimetric arrays typically have an exceptional selectivity to the target analyte if the right colorimetric dyes are chosen. We present a sensor system consisting of a Capacitive Micromachined Ultrasonic Transducer (CMUT) and a colorimetric array for detection of phenylacetone. The CMUT is used as a resonant gravimetric gas sensor where the resonance frequency shift due to mass loading of the plate. A single Local Oxidation of Silicon (LOCOS) step was used to define the cavities which were sealed with a Si3N4 plate with a thickness of 100nm, resulting in a resonance frequency of 38:8MHz and a theoretical mass sensitivity of 28:3 zg/Hz·μ2. The CMUTs were functionalized with the same dyes used to fabricate colorimetric arrays. While both the CMUTs and the colorimetric arrays showed selectivity to phenylacetone, the best selectivity was achieved by the colorimetric array. Furthermore, the mass of the phenylacetone was found as a function of time. Thus, the combination of the colorimetric array and the CMUT results in a good selectivity and a quantitative value for the mass.",
    author = "M{\o}lgaard, {Mathias Johannes Gr{\o}ndahl} and Milan Laustsen and Thygesen, {Ida Lysgaard} and Jakobsen, {Mogens Havsteen} and Andresen, {Thomas Lars} and Thomsen, {Erik Vilain}",
    year = "2017",
    doi = "10.1109/ULTSYM.2017.8091676",
    language = "English",
    booktitle = "2017 IEEE International Ultrasonics Symposium (IUS)",
    publisher = "IEEE",
    address = "United States",

    }

    Mølgaard, MJG, Laustsen, M, Thygesen, IL, Jakobsen, MH, Andresen, TL & Thomsen, EV 2017, Combined Colorimetric and Gravimetric CMUT Sensor for Detection of Phenylacetone. in 2017 IEEE International Ultrasonics Symposium (IUS). IEEE, 2017 IEEE International Ultrasonics Symposium (IUS), Washington, United States, 06/09/2017. https://doi.org/10.1109/ULTSYM.2017.8091676

    Combined Colorimetric and Gravimetric CMUT Sensor for Detection of Phenylacetone. / Mølgaard, Mathias Johannes Grøndahl; Laustsen, Milan; Thygesen, Ida Lysgaard; Jakobsen, Mogens Havsteen; Andresen, Thomas Lars; Thomsen, Erik Vilain.

    2017 IEEE International Ultrasonics Symposium (IUS). IEEE, 2017.

    Research output: Chapter in Book/Report/Conference proceedingArticle in proceedingsResearchpeer-review

    TY - GEN

    T1 - Combined Colorimetric and Gravimetric CMUT Sensor for Detection of Phenylacetone

    AU - Mølgaard, Mathias Johannes Grøndahl

    AU - Laustsen, Milan

    AU - Thygesen, Ida Lysgaard

    AU - Jakobsen, Mogens Havsteen

    AU - Andresen, Thomas Lars

    AU - Thomsen, Erik Vilain

    PY - 2017

    Y1 - 2017

    N2 - The detection of phenylacetone is of interest as it is a common precursor for the synthesis of (meth)amphetamine. Resonant gravimetric sensors can be used to detect the mass and hereby the concentration of a gas while colorimetric arrays typically have an exceptional selectivity to the target analyte if the right colorimetric dyes are chosen. We present a sensor system consisting of a Capacitive Micromachined Ultrasonic Transducer (CMUT) and a colorimetric array for detection of phenylacetone. The CMUT is used as a resonant gravimetric gas sensor where the resonance frequency shift due to mass loading of the plate. A single Local Oxidation of Silicon (LOCOS) step was used to define the cavities which were sealed with a Si3N4 plate with a thickness of 100nm, resulting in a resonance frequency of 38:8MHz and a theoretical mass sensitivity of 28:3 zg/Hz·μ2. The CMUTs were functionalized with the same dyes used to fabricate colorimetric arrays. While both the CMUTs and the colorimetric arrays showed selectivity to phenylacetone, the best selectivity was achieved by the colorimetric array. Furthermore, the mass of the phenylacetone was found as a function of time. Thus, the combination of the colorimetric array and the CMUT results in a good selectivity and a quantitative value for the mass.

    AB - The detection of phenylacetone is of interest as it is a common precursor for the synthesis of (meth)amphetamine. Resonant gravimetric sensors can be used to detect the mass and hereby the concentration of a gas while colorimetric arrays typically have an exceptional selectivity to the target analyte if the right colorimetric dyes are chosen. We present a sensor system consisting of a Capacitive Micromachined Ultrasonic Transducer (CMUT) and a colorimetric array for detection of phenylacetone. The CMUT is used as a resonant gravimetric gas sensor where the resonance frequency shift due to mass loading of the plate. A single Local Oxidation of Silicon (LOCOS) step was used to define the cavities which were sealed with a Si3N4 plate with a thickness of 100nm, resulting in a resonance frequency of 38:8MHz and a theoretical mass sensitivity of 28:3 zg/Hz·μ2. The CMUTs were functionalized with the same dyes used to fabricate colorimetric arrays. While both the CMUTs and the colorimetric arrays showed selectivity to phenylacetone, the best selectivity was achieved by the colorimetric array. Furthermore, the mass of the phenylacetone was found as a function of time. Thus, the combination of the colorimetric array and the CMUT results in a good selectivity and a quantitative value for the mass.

    U2 - 10.1109/ULTSYM.2017.8091676

    DO - 10.1109/ULTSYM.2017.8091676

    M3 - Article in proceedings

    BT - 2017 IEEE International Ultrasonics Symposium (IUS)

    PB - IEEE

    ER -