Characterization of La1-xSrxMnO3±d (x = 0.15, d 0) and La1-xSrxCrO3±d (x = 0.2, d 0) Powders by X-ray Powder Diffraction

Rolf Berg, Mette M. Andersen, Niels Bjerrum

Research output: Chapter in Book/Report/Conference proceedingArticle in proceedingsResearch

Abstract

La1-xSrxMnO3 ± d (x = 0.15, d 0) and La1-xSrxCrO3 ± d (x= 0.2, d 0) powders were synthesized by drip/spray pyrolysis of solutions of analysed metal nitrate mixtures, with added chelating ligands and solvents. The solutions were dripped or sprayed into a rotating tube furnace at 600-700 oC, resulting in homogeneous single phased ceramic powders. X-ray diffraction diagrams were taken using copper Ka radiation with a Bragg-Brentano diffractometer. The obtained X-ray diagrams of the synthesised La0.85Sr0.15MnO3±d and La0.8Sr0.2CrO3±d (d 0) powders were compared to data in the literature which was reviewed. The structure, lattice parameters, etc., of the resulting phases do not depend very much on the kind of chelating agent but on the metal composition and the history of the sample.
Original languageEnglish
Title of host publication2nd European Solid Oxide Fuel Cell Forum
Place of PublicationOberrohrdorf
PublisherUlf Bossel
Publication date1996
Pages413-422
Publication statusPublished - 1996
Event2nd European Solid Oxide Fuel Cell Forum - Oslo, Norway
Duration: 6 May 199610 May 1996

Conference

Conference2nd European Solid Oxide Fuel Cell Forum
CountryNorway
CityOslo
Period06/05/199610/05/1996

Cite this

Berg, R., Andersen, M. M., & Bjerrum, N. (1996). Characterization of La1-xSrxMnO3±d (x = 0.15, d 0) and La1-xSrxCrO3±d (x = 0.2, d 0) Powders by X-ray Powder Diffraction. In 2nd European Solid Oxide Fuel Cell Forum (pp. 413-422). Ulf Bossel.