An alternative preparation method for ion exchanged catalysts: Solid state redox reaction

E. Schneider, A. Hagen, J.-D. Grunwaldt, F. Roessner

    Research output: Chapter in Book/Report/Conference proceedingArticle in proceedingsResearch

    Abstract

    A new method for modifying zeolites with zinc is proposed. The solid state redox reaction between metallic zinc and ZSM-5 zeolites with different Si/Al ratios was investigated by temperature programmed hydrogen evolution (TPHE), X-ray absorption near edge structure (XANES) and diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS). The evolution of hydrogen was detected at temperatures above 620 K. The source of hydrogen was the solid state redox reaction of the metal with protons of the support. The samples exhibit catalytic activity in ethane aromatization indicating that zinc should be located at the same sites as in catalysts prepared by conventional methods. Combination of XANES and catalytic activity point to zinc being mainly present in tetrahedral geometry under reaction conditions.
    Original languageEnglish
    Title of host publicationRecent advances in the science and technology of zeolites and related materials : pts. A,B,C
    EditorsE. van Steen, L.H. Callanan, M. Claeys
    Place of PublicationOxford
    PublisherElsevier
    Publication date2004
    Pages2192-2199
    ISBN (Print)0-444-51805-3
    Publication statusPublished - 2004
    Event14th International Zeolite Conference - Cape Town, South Africa
    Duration: 25 Apr 200430 Apr 2004

    Conference

    Conference14th International Zeolite Conference
    Country/TerritorySouth Africa
    CityCape Town
    Period25/04/200430/04/2004
    SeriesStudies in Surface Science and Catalysis, 154

    Keywords

    • solid state redox reaction
    • zinc
    • ZSM-5
    • DRIFTS
    • TPHE
    • XANES
    • ethane
    • aromatization

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