A new synthesis of aliphatic isothiocyanates from primary amines, convenient for in situ use

Ulrik Boas, M. H. Jakobsen

    Research output: Contribution to journalJournal articleResearchpeer-review

    Abstract

    Primary aliphatic amines react with carbon disulfide in the presence of BOP (benzotriazole-1-yl-oxy-tris(dimethylamino)phosphonium hexafluorophosphate 1, giving the corresponding isothiocyanates in good to high yields and high purity; a number of isothiocyanates are synthesized and isolated or generated in situ and treated with a nucleophile.
    Original languageEnglish
    JournalJournal of the Chemical Society D: Chemical Communications
    Issue number19
    Pages (from-to)1995-1996
    ISSN0022-4936
    DOIs
    Publication statusPublished - 1995

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