A laser heating facility for energy-dispersive X-ray absorption spectroscopy

Innokenty Kantor, C. Marini, O. Mathon, S. Pascarelli

Research output: Contribution to journalJournal articleResearchpeer-review

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Abstract

A double-sided laser heating setup for diamond anvil cells installed on the ID24 beamline of the ESRF is presented here. The setup geometry is specially adopted for the needs of energy-dispersive X-ray absorption spectroscopic (XAS) studies of materials under extreme pressure and temperature conditions. We illustrate the performance of the facility with a study on metallic nickel at 60 GPa. The XAS data provide the temperature of the melting onset and quantitative information on the structural parameters of the first coordination shell in the hot solid up to melting.
Original languageEnglish
Article number013111
JournalReview of Scientific Instruments
Volume89
Issue number1
Number of pages13
ISSN0034-6748
DOIs
Publication statusPublished - 2018

Keywords

  • Laser applications
  • X-ray absorption spectroscopy
  • Transition
  • Diamond-anvil
  • Absorption spectra

Cite this

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title = "A laser heating facility for energy-dispersive X-ray absorption spectroscopy",
abstract = "A double-sided laser heating setup for diamond anvil cells installed on the ID24 beamline of the ESRF is presented here. The setup geometry is specially adopted for the needs of energy-dispersive X-ray absorption spectroscopic (XAS) studies of materials under extreme pressure and temperature conditions. We illustrate the performance of the facility with a study on metallic nickel at 60 GPa. The XAS data provide the temperature of the melting onset and quantitative information on the structural parameters of the first coordination shell in the hot solid up to melting.",
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A laser heating facility for energy-dispersive X-ray absorption spectroscopy. / Kantor, Innokenty; Marini, C.; Mathon, O.; Pascarelli, S.

In: Review of Scientific Instruments, Vol. 89, No. 1, 013111, 2018.

Research output: Contribution to journalJournal articleResearchpeer-review

TY - JOUR

T1 - A laser heating facility for energy-dispersive X-ray absorption spectroscopy

AU - Kantor, Innokenty

AU - Marini, C.

AU - Mathon, O.

AU - Pascarelli, S.

PY - 2018

Y1 - 2018

N2 - A double-sided laser heating setup for diamond anvil cells installed on the ID24 beamline of the ESRF is presented here. The setup geometry is specially adopted for the needs of energy-dispersive X-ray absorption spectroscopic (XAS) studies of materials under extreme pressure and temperature conditions. We illustrate the performance of the facility with a study on metallic nickel at 60 GPa. The XAS data provide the temperature of the melting onset and quantitative information on the structural parameters of the first coordination shell in the hot solid up to melting.

AB - A double-sided laser heating setup for diamond anvil cells installed on the ID24 beamline of the ESRF is presented here. The setup geometry is specially adopted for the needs of energy-dispersive X-ray absorption spectroscopic (XAS) studies of materials under extreme pressure and temperature conditions. We illustrate the performance of the facility with a study on metallic nickel at 60 GPa. The XAS data provide the temperature of the melting onset and quantitative information on the structural parameters of the first coordination shell in the hot solid up to melting.

KW - Laser applications

KW - X-ray absorption spectroscopy

KW - Transition

KW - Diamond-anvil

KW - Absorption spectra

U2 - 10.1063/1.5010345

DO - 10.1063/1.5010345

M3 - Journal article

C2 - 29390671

VL - 89

JO - Review of Scientific Instruments

JF - Review of Scientific Instruments

SN - 0034-6748

IS - 1

M1 - 013111

ER -