TY - JOUR

T1 - Confirmatory analysis of steroids in muscle using liquid chromatography-tandem mass spectrometry

A1 - Pedersen,Mikael

A1 - Andersen,Jens Hinge

AU - Pedersen,Mikael

AU - Andersen,Jens Hinge

PB - Taylor & Francis Ltd.

PY - 2011

Y1 - 2011

N2 - A method is described for screening and confirmation of synthetic and endogenous steroids in muscle tissue. The method is sensitive, selective, and rapid and the consumption of organic solvents is low, compared to previously published methods. The procedure involves hydrolysis, defattening with heptane and final clean up with SPE using C18 cartridge. After filtration, the analytes are analysed by LC/MS/MS and quantification is performed using deuterated internal standards. Decision limits (CCα) varied from 0.02 to 0.33 μg kg-1 and the detection capabilities (CCβ) were

AB - A method is described for screening and confirmation of synthetic and endogenous steroids in muscle tissue. The method is sensitive, selective, and rapid and the consumption of organic solvents is low, compared to previously published methods. The procedure involves hydrolysis, defattening with heptane and final clean up with SPE using C18 cartridge. After filtration, the analytes are analysed by LC/MS/MS and quantification is performed using deuterated internal standards. Decision limits (CCα) varied from 0.02 to 0.33 μg kg-1 and the detection capabilities (CCβ) were

U2 - 10.1080/19440049.2010.549153

DO - 10.1080/19440049.2010.549153

JO - Food Additives and Contaminants

JF - Food Additives and Contaminants

SN - 0265-203X

IS - 4

VL - 28

SP - 428

EP - 437

ER -